TA Instruments

AR1701-0001f

04/09/2012 15:46:39

Sample name	ASW 10 mm from base, 60 mm to top, disk 4 PMMA+Br clean
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1701
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 15:46:39

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

17.46	5.131	3.403	1.0040	22.4	770.4	3.2971	10000	0.1891	29.27	4.1214	412.14	3.383E-3	0.0	1.0	61.004	53.558	4.105
0.8220	13.19	0.06232	2.0280	22.4	791.9	14.4496	10000	0.1944	4.552	18.062	1806.2	3.384E-3	0.0	1.0	62.028	2.5217	10.55
1.596	19.82	0.08052	3.0360	22.4	790.3	28.0366	10000	0.1940	2.012	35.046	3504.6	3.383E-3	0.1	1.1	63.036	4.8954	15.85
2.161	23.41	0.09233	4.0280	22.4	785.3	41.9330	10000	0.1927	1.433	52.416	5241.6	3.384E-3	0.1	1.1	64.028	6.6312	18.73
3.325	31.11	0.1069	5.0280	22.4	782.0	68.6288	10000	0.1919	0.8078	85.786	8578.6	3.384E-3	0.1	1.1	65.028	10.201	24.89
5.195	39.69	0.1309	6.0160	22.4	785.3	107.8930	10000	0.1927	0.4985	134.87	13487	3.384E-3	0.1	1.1	66.016	15.938	31.75
6.077	42.73	0.1422	7.0280	22.4	790.3	127.4740	10000	0.1940	0.4329	159.34	15934	3.383E-3	0.1	1.1	67.028	18.643	34.18
7.414	49.29	0.1504	8.0280	22.4	789.5	166.2370	10000	0.1938	0.3250	207.80	20780	3.383E-3	0.1	1.1	68.028	22.747	39.43
9.721	57.67	0.1686	9.0040	22.4	784.5	224.0970	10000	0.1925	0.2359	280.12	28012	3.384E-3	0.2	1.2	69.004	29.825	46.13
11.75	63.81	0.1841	10.036	22.4	775.4	275.6880	10000	0.1903	0.1904	344.61	34461	3.384E-3	0.2	1.2	70.036	36.034	51.05
13.60	69.76	0.1949	11.036	22.4	783.7	327.0400	10000	0.1923	0.1610	408.80	40880	3.384E-3	0.2	1.2	71.036	41.711	55.81
15.40	75.22	0.2047	12.004	22.4	759.7	378.1800	10000	0.1865	0.1343	472.73	47273	3.384E-3	0.2	1.2	72.004	47.250	60.18
17.39	80.61	0.2157	13.032	22.4	777.9	435.6810	10000	0.1909	0.1197	544.60	54460	3.384E-3	0.2	1.2	73.032	53.338	64.48
20.59	89.32	0.2305	14.044	22.4	776.2	532.3350	10000	0.1905	0.09729	665.42	66542	3.384E-3	0.2	1.2	74.044	63.158	71.46
22.53	94.68	0.2379	15.036	22.4	762.2	595.0460	10000	0.1871	0.08503	743.81	74381	3.384E-3	0.3	1.3	75.036	69.109	75.74
24.78	99.98	0.2478	16.028	22.4	762.2	665.2090	10000	0.1871	0.07624	831.51	83151	3.384E-3	0.3	1.3	76.028	76.022	79.99
27.03	105.7	0.2557	17.028	22.4	753.1	741.7350	10000	0.1848	0.06737	927.17	92717	3.383E-3	0.3	1.3	77.028	82.935	84.58
30.40	113.8	0.2672	18.028	22.4	744.8	855.8800	10000	0.1828	0.05752	1069.9	1.0699E5	3.384E-3	0.3	1.3	78.028	93.264	91.03
32.25	118.9	0.2714	19.008	22.4	759.7	932.0840	10000	0.1865	0.05378	1165.1	1.1651E5	3.384E-3	0.3	1.3	79.008	98.950	95.08
34.87	124.3	0.2805	20.004	22.4	753.1	1020.9800	10000	0.1848	0.04874	1276.2	1.2762E5	3.384E-3	0.3	1.3	80.004	106.99	99.44
38.66	132.3	0.2921	21.008	22.4	756.4	1154.2700	10000	0.1856	0.04319	1442.8	1.4428E5	3.384E-3	0.4	1.4	81.008	118.60	105.9
41.15	137.4	0.2994	22.028	22.4	744.0	1243.0900	10000	0.1826	0.03939	1553.9	1.5539E5	3.384E-3	0.4	1.4	82.028	126.24	109.9
43.72	142.8	0.3061	23.028	22.4	739.0	1344.4800	10000	0.1814	0.03622	1680.6	1.6806E5	3.384E-3	0.4	1.4	83.028	134.14	114.3
47.67	150.9	0.3160	24.004	22.4	727.5	1496.5800	10000	0.1785	0.03196	1870.7	1.8707E5	3.384E-3	0.4	1.4	84.004	146.26	120.7
50.29	156.0	0.3224	25.028	22.4	718.4	1598.6500	10000	0.1763	0.02953	1998.3	1.9983E5	3.383E-3	0.4	1.4	85.028	154.27	124.8
52.81	161.4	0.3272	26.004	22.4	717.5	1711.9301	10000	0.1761	0.02756	2139.9	2.1399E5	3.384E-3	0.4	1.4	86.004	162.01	129.1
57.17	169.4	0.3376	27.004	22.4	723.3	1882.8500	10000	0.1775	0.02522	2353.6	2.3536E5	3.384E-3	0.5	1.5	87.004	175.40	135.5
60.40	174.5	0.3461	28.000	22.4	717.5	1996.7400	10000	0.1761	0.02357	2495.9	2.4959E5	3.383E-3	0.5	1.5	88.000	185.29	139.6
62.92	179.6	0.3503	29.004	22.4	713.4	2117.0200	10000	0.1751	0.02212	2646.3	2.6463E5	3.384E-3	0.5	1.5	89.004	193.03	143.7
68.22	187.6	0.3637	30.028	22.4	690.3	2306.7100	10000	0.1694	0.01961	2883.4	2.8834E5	3.384E-3	0.5	1.5	90.028	209.31	150.1
71.52	192.7	0.3711	31.028	22.4	698.5	2433.1799	10000	0.1714	0.01880	3041.5	3.0415E5	3.384E-3	0.5	1.5	91.028	219.41	154.2
75.40	200.6	0.3759	32.032	22.4	709.3	2636.3501	10000	0.1741	0.01763	3295.4	3.2954E5	3.383E-3	0.5	1.5	92.032	231.32	160.5
78.59	205.9	0.3818	33.004	22.4	698.5	2775.4099	10000	0.1714	0.01648	3469.3	3.4693E5	3.383E-3	0.6	1.6	93.004	241.10	164.7
81.71	211.0	0.3872	34.028	22.4	682.0	2914.8899	10000	0.1674	0.01532	3643.6	3.6436E5	3.384E-3	0.6	1.6	94.028	250.68	168.8
87.46	218.6	0.4000	35.004	22.4	684.5	3129.2100	10000	0.1680	0.01432	3911.5	3.9115E5	3.384E-3	0.6	1.6	95.004	268.32	174.9
89.42	223.9	0.3993	36.028	22.4	675.4	3280.0200	10000	0.1658	0.01347	4100.0	4.1000E5	3.384E-3	0.6	1.6	96.028	274.33	179.1
94.65	229.1	0.4131	37.004	22.4	686.9	3431.6399	10000	0.1686	0.01309	4289.6	4.2896E5	3.384E-3	0.6	1.6	97.004	290.37	183.3
98.73	236.7	0.4172	38.028	22.4	663.0	3659.2800	10000	0.1627	0.01184	4574.1	4.5741E5	3.384E-3	0.6	1.6	98.028	302.89	189.3
101.6	241.9	0.4201	39.028	22.4	644.8	3823.2300	10000	0.1583	0.01102	4779.0	4.7790E5	3.384E-3	0.7	1.7	99.028	311.72	193.5
106.7	249.6	0.4276	40.028	22.4	644.8	4069.3999	10000	0.1583	0.01035	5086.8	5.0868E5	3.384E-3	0.7	1.7	100.028	327.47	199.7
110.1	254.6	0.4325	41.036	22.4	653.9	4233.6299	10000	0.1605	0.01008	5292.0	5.2920E5	3.384E-3	0.7	1.7	101.036	337.87	203.7
117.4	262.5	0.4471	42.028	22.4	627.4	4500.4600	10000	0.1540	9.107E-3	5625.6	5.6256E5	3.383E-3	0.7	1.7	102.028	360.07	210.0
120.5	267.6	0.4503	43.004	22.4	662.1	4675.5400	10000	0.1625	9.244E-3	5844.4	5.8444E5	3.383E-3	0.7	1.7	103.004	369.73	214.1
124.7	272.7	0.4573	44.028	22.4	652.2	4852.1299	10000	0.1601	8.771E-3	6065.2	6.0652E5	3.383E-3	0.7	1.7	104.028	382.58	218.2
130.2	280.4	0.4643	45.040	22.4	623.3	5129.7798	10000	0.1530	7.929E-3	6412.2	6.4122E5	3.384E-3	0.8	1.8	105.040	399.38	224.3
133.8	285.6	0.4687	46.004	22.4	633.2	5319.2500	10000	0.1554	7.766E-3	6649.1	6.6491E5	3.384E-3	0.8	1.8	106.004	410.58	228.4
140.3	293.1	0.4787	47.028	22.4	624.1	5603.0498	10000	0.1532	7.263E-3	7003.8	7.0038E5	3.383E-3	0.8	1.8	107.028	430.49	234.5
143.9	298.2	0.4827	48.016	22.4	600.2	5799.6802	10000	0.1473	6.750E-3	7249.6	7.2496E5	3.383E-3	0.8	1.8	108.016	441.52	238.5
146.2	303.4	0.4818	49.004	22.4	640.7	6000.7002	10000	0.1572	6.962E-3	7500.9	7.5009E5	3.384E-3	0.8	1.8	109.004	448.44	242.7
152.4	311.0	0.4901	50.028	22.4	637.3	6305.0200	10000	0.1564	6.590E-3	7881.3	7.8813E5	3.383E-3	0.8	1.8	110.028	467.63	248.8
156.6	316.0	0.4955	51.028	22.4	620.8	6511.4600	10000	0.1524	6.216E-3	8139.3	8.1393E5	3.384E-3	0.9	1.9	111.028	480.44	252.8
165.1	323.8	0.5099	52.004	22.4	573.7	6833.0498	10000	0.1408	5.472E-3	8541.3	8.5413E5	3.384E-3	0.9	1.9	112.004	506.52	259.0
166.8	328.9	0.5071	53.004	22.4	604.3	7047.6201	10000	0.1483	5.586E-3	8809.5	8.8095E5	3.383E-3	0.9	1.9	113.004	511.64	263.1
172.8	336.4	0.5137	54.004	22.4	615.0	7375.3501	10000	0.1510	5.433E-3	9219.2	9.2192E5	3.384E-3	0.9	1.9	114.004	530.26	269.2
180.1	341.6	0.5272	55.028	22.4	627.4	7603.5400	10000	0.1540	5.376E-3	9504.4	9.5044E5	3.383E-3	0.9	1.9	115.028	552.55	273.3
182.1	346.7	0.5251	56.028	22.4	607.6	7943.9302	10000	0.1491	5.054E-3	9929.9	9.9299E5	3.384E-3	0.9	1.9	116.028	558.53	277.4
190.3	354.2	0.5372	57.004	22.4	564.6	8169.7798	10000	0.1386	4.500E-3	10212	1.0212E6	3.384E-3	1.0	2.0	117.004	583.82	283.4
195.6	359.4	0.5443	58.004	22.4	567.9	8414.9102	10000	0.1394	4.398E-3	10519	1.0519E6	3.384E-3	1.0	2.0	118.004	600.12	287.5
202.0	367.0	0.5503	59.004	22.4	552.2	8768.7305	10000	0.1355	4.100E-3	10961	1.0961E6	3.384E-3	1.0	2.0	119.004	619.66	293.6
206.8	372.0	0.5558	60.028	22.4	552.2	9008.0703	10000	0.1355	3.990E-3	11260	1.1260E6	3.383E-3	1.0	2.0	120.028	634.39	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

209.9	375.0	0.5599	1.0000	22.4	567.1	307.3890	10000	0.1392	4.033E-3	384.24	38424	3.383E-3	0.0	2.0	122.000	644.11	300.0
207.0	375.0	0.5521	2.0120	22.4	547.2	559.0820	10000	0.1343	3.891E-3	698.85	69885	3.383E-3	0.0	2.1	123.012	635.22	300.0
207.4	375.0	0.5530	3.0120	22.4	542.3	809.2600	10000	0.1331	3.856E-3	1011.6	1.0116E5	3.383E-3	0.1	2.1	124.012	636.17	300.0
208.9	375.0	0.5572	4.0080	22.4	552.2	1186.0200	10000	0.1355	3.927E-3	1482.5	1.4825E5	3.384E-3	0.1	2.1	125.008	641.02	300.0
209.4	375.0	0.5583	4.9960	22.4	550.5	1437.1200	10000	0.1351	3.915E-3	1796.4	1.7964E5	3.384E-3	0.1	2.1	125.996	642.28	300.0
207.8	375.0	0.5542	6.0160	22.4	576.2	1814.1700	10000	0.1414	4.097E-3	2267.7	2.2677E5	3.384E-3	0.1	2.1	127.016	637.64	300.0
211.4	375.0	0.5639	6.9960	22.4	524.1	2065.5701	10000	0.1286	3.727E-3	2582.0	2.5820E5	3.384E-3	0.1	2.1	127.996	648.70	300.0
210.3	375.0	0.5608	8.0040	22.4	549.7	2323.5200	10000	0.1349	3.909E-3	2904.4	2.9044E5	3.384E-3	0.1	2.2	129.004	645.22	300.0
210.6	375.0	0.5616	9.0120	22.4	566.3	2693.6799	10000	0.1390	4.027E-3	3367.1	3.3671E5	3.384E-3	0.2	2.2	130.012	646.15	300.0
210.0	375.0	0.5601	10.012	22.4	526.6	2945.1799	10000	0.1292	3.744E-3	3681.5	3.6815E5	3.384E-3	0.2	2.2	131.012	644.37	300.0
208.5	375.0	0.5559	11.016	22.4	535.7	3325.7200	10000	0.1315	3.809E-3	4157.2	4.1572E5	3.384E-3	0.2	2.2	132.016	639.53	300.0
207.5	375.0	0.5534	12.012	22.4	551.4	3573.4600	10000	0.1353	3.921E-3	4466.8	4.4668E5	3.384E-3	0.2	2.2	133.012	636.62	300.0
208.4	375.0	0.5558	13.012	22.4	518.3	3824.7700	10000	0.1272	3.686E-3	4781.0	4.7810E5	3.384E-3	0.2	2.2	134.012	639.43	300.0
211.9	375.0	0.5652	13.996	22.4	528.2	4201.6802	10000	0.1296	3.756E-3	5252.1	5.2521E5	3.383E-3	0.2	2.2	134.996	650.20	300.0
210.0	375.0	0.5600	14.996	22.4	552.2	4453.1699	10000	0.1355	3.927E-3	5566.5	5.5665E5	3.384E-3	0.2	2.3	135.996	644.23	300.0
209.1	375.0	0.5577	16.012	22.4	569.6	4720.0298	10000	0.1398	4.050E-3	5900.0	5.9000E5	3.384E-3	0.3	2.3	137.012	641.64	300.0
206.1	375.0	0.5497	17.012	22.4	588.6	5081.4902	10000	0.1445	4.186E-3	6351.9	6.3519E5	3.384E-3	0.3	2.3	138.012	632.41	300.0
209.1	375.0	0.5577	18.004	22.4	565.4	5332.7998	10000	0.1388	4.021E-3	6666.0	6.6660E5	3.384E-3	0.3	2.3	139.004	641.58	300.0
208.5	375.0	0.5561	19.012	22.4	547.2	5709.6299	10000	0.1343	3.892E-3	7137.0	7.1370E5	3.383E-3	0.3	2.3	140.012	639.73	300.0
207.7	375.0	0.5539	19.996	22.4	562.1	5960.9199	10000	0.1380	3.997E-3	7451.2	7.4512E5	3.383E-3	0.3	2.3	140.996	637.24	300.0
207.1	375.0	0.5523	20.996	22.4	581.1	6214.3301	10000	0.1426	4.133E-3	7767.9	7.7679E5	3.384E-3	0.3	2.4	141.996	635.37	300.0
207.6	375.0	0.5537	22.012	22.4	570.4	6589.3599	10000	0.1400	4.056E-3	8236.7	8.2367E5	3.384E-3	0.4	2.4	143.012	637.01	300.0
207.8	375.0	0.5540	23.012	22.4	534.8	6840.7500	10000	0.1313	3.803E-3	8550.9	8.5509E5	3.384E-3	0.4	2.4	144.012	637.41	300.0
209.1	375.0	0.5576	24.012	22.4	563.0	7219.1401	10000	0.1382	4.003E-3	9023.9	9.0239E5	3.383E-3	0.4	2.4	145.012	641.53	300.0
205.9	375.0	0.5489	25.012	22.4	588.6	7472.4102	10000	0.1445	4.185E-3	9340.5	9.3405E5	3.383E-3	0.4	2.4	146.012	631.56	300.0
210.3	375.0	0.5607	26.012	22.4	545.6	7720.2798	10000	0.1339	3.880E-3	9650.4	9.6504E5	3.383E-3	0.4	2.5	147.012	645.11	300.0
208.9	375.0	0.5571	26.996	22.4	559.6	8097.2100	10000	0.1374	3.980E-3	10122	1.0122E6	3.383E-3	0.4	2.5	147.996	640.88	300.0
207.0	375.0	0.5520	28.012	22.4	544.8	8348.5996	10000	0.1337	3.874E-3	10436	1.0436E6	3.384E-3	0.5	2.5	149.012	635.03	300.0
208.8	375.0	0.5568	29.012	22.4	528.2	8601.1201	10000	0.1296	3.756E-3	10751	1.0751E6	3.383E-3	0.5	2.5	150.012	640.63	300.0
207.0	375.0	0.5519	30.012	22.4	594.4	8976.8604	10000	0.1459	4.227E-3	11221	1.1221E6	3.383E-3	0.5	2.5	151.012	635.01	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

205.6	372.3	0.5524	1.0000	22.4	572.9	212.7530	10000	0.1406	4.134E-3	265.94	26594	3.384E-3	0.0	2.5	152.000	630.92	297.8
200.1	364.7	0.5487	2.1840	22.4	574.5	569.6730	10000	0.1410	4.319E-3	712.09	71209	3.384E-3	0.0	2.6	153.184	613.96	291.8
195.9	359.6	0.5447	3.0000	22.4	582.0	807.6770	10000	0.1428	4.500E-3	1009.6	1.0096E5	3.383E-3	0.1	2.6	154.000	600.97	287.7
188.5	351.9	0.5355	4.0000	22.4	570.4	1158.2700	10000	0.1400	4.605E-3	1447.8	1.4478E5	3.383E-3	0.1	2.6	155.000	578.21	281.5
184.3	346.9	0.5311	5.0440	22.4	567.9	1384.9700	10000	0.1394	4.718E-3	1731.2	1.7312E5	3.384E-3	0.1	2.6	156.044	565.28	277.6
177.0	339.3	0.5215	6.0040	22.4	618.3	1721.8500	10000	0.1518	5.370E-3	2152.3	2.1523E5	3.384E-3	0.1	2.6	157.004	542.90	271.5
171.8	334.2	0.5141	7.0160	22.4	612.5	1947.1700	10000	0.1503	5.486E-3	2434.0	2.4340E5	3.383E-3	0.1	2.6	158.016	527.02	267.3
168.5	329.1	0.5119	8.0000	22.4	603.5	2160.1399	10000	0.1481	5.571E-3	2700.2	2.7002E5	3.384E-3	0.1	2.7	159.000	516.83	263.3
163.1	321.5	0.5074	9.0040	22.4	582.8	2479.2900	10000	0.1430	5.638E-3	3099.1	3.0991E5	3.383E-3	0.2	2.7	160.004	500.49	257.2
158.7	316.4	0.5015	10.024	22.4	624.1	2694.8601	10000	0.1532	6.236E-3	3368.6	3.3686E5	3.384E-3	0.2	2.7	161.024	486.76	253.1
152.0	308.7	0.4923	11.016	22.4	632.4	2998.8501	10000	0.1552	6.637E-3	3748.6	3.7486E5	3.384E-3	0.2	2.7	162.016	466.23	246.9
146.8	303.6	0.4835	12.000	22.4	641.5	3199.2300	10000	0.1574	6.958E-3	3999.0	3.9990E5	3.384E-3	0.2	2.7	163.000	450.39	242.9
144.4	295.9	0.4882	13.004	22.4	634.9	3500.5200	10000	0.1558	7.252E-3	4375.7	4.3757E5	3.384E-3	0.2	2.7	164.004	443.17	236.7
140.1	290.8	0.4816	14.000	22.4	607.6	3687.3401	10000	0.1491	7.183E-3	4609.2	4.6092E5	3.383E-3	0.2	2.8	165.000	429.71	232.7
135.4	285.8	0.4737	15.000	22.4	659.7	3876.6101	10000	0.1619	8.075E-3	4845.8	4.8458E5	3.383E-3	0.3	2.8	166.000	415.35	228.6
127.5	278.1	0.4586	16.000	22.4	661.3	4156.5801	10000	0.1623	8.552E-3	5195.7	5.1957E5	3.384E-3	0.3	2.8	167.000	391.23	222.5
123.1	272.9	0.4509	17.004	22.4	663.0	4337.8501	10000	0.1627	8.901E-3	5422.3	5.4223E5	3.384E-3	0.3	2.8	168.004	377.52	218.3
118.6	265.4	0.4469	18.004	22.4	660.5	4602.3101	10000	0.1621	9.380E-3	5752.9	5.7529E5	3.384E-3	0.3	2.8	169.004	363.80	212.3
115.3	260.2	0.4430	19.004	22.4	653.1	4775.6299	10000	0.1603	9.645E-3	5969.5	5.9695E5	3.384E-3	0.3	2.8	170.004	353.66	208.2
109.5	252.4	0.4341	20.016	22.4	658.0	5035.0698	10000	0.1615	0.01033	6293.8	6.2938E5	3.384E-3	0.3	2.9	171.016	336.07	201.9
106.0	247.3	0.4285	21.004	22.4	673.7	5194.6201	10000	0.1654	0.01101	6493.3	6.4933E5	3.384E-3	0.4	2.9	172.004	325.14	197.9
101.6	242.2	0.4194	22.000	22.4	677.0	5357.9902	10000	0.1662	0.01154	6697.5	6.6975E5	3.384E-3	0.4	2.9	173.000	311.62	193.8
97.20	234.4	0.4147	23.000	22.4	678.7	5594.8398	10000	0.1666	0.01235	6993.6	6.9936E5	3.384E-3	0.4	2.9	174.000	298.20	187.5
93.32	229.4	0.4069	24.020	22.4	685.3	5745.5098	10000	0.1682	0.01302	7181.9	7.1819E5	3.384E-3	0.4	2.9	175.020	286.31	183.5
89.17	221.7	0.4023	25.004	22.4	679.5	5969.8198	10000	0.1668	0.01383	7462.3	7.4623E5	3.384E-3	0.4	2.9	176.004	273.57	177.3
84.62	216.4	0.3911	26.004	22.4	685.3	6123.3398	10000	0.1682	0.01464	7654.2	7.6542E5	3.384E-3	0.4	3.0	177.004	259.61	173.1
82.48	211.3	0.3904	27.004	22.4	698.5	6257.1001	10000	0.1714	0.01565	7821.4	7.8214E5	3.383E-3	0.5	3.0	178.004	253.05	169.0
77.28	203.6	0.3796	28.004	22.4	703.5	6463.2100	10000	0.1727	0.01697	8079.0	8.0790E5	3.384E-3	0.5	3.0	179.004	237.10	162.9
74.45	198.3	0.3754	29.004	22.4	687.8	6600.7100	10000	0.1688	0.01749	8250.9	8.2509E5	3.384E-3	0.5	3.0	180.004	228.40	158.6
70.65	193.0	0.3661	30.000	22.4	725.0	6732.3501	10000	0.1779	0.01947	8415.4	8.4154E5	3.384E-3	0.5	3.0	181.000	216.74	154.4
66.81	185.3	0.3605	31.000	22.4	709.3	6919.0898	10000	0.1741	0.02065	8648.9	8.6489E5	3.384E-3	0.5	3.0	182.000	204.96	148.3
63.35	180.0	0.3519	32.016	22.4	712.6	7043.7900	10000	0.1749	0.02198	8804.7	8.8047E5	3.383E-3	0.5	3.1	183.016	194.36	144.0
58.43	172.2	0.3393	33.000	22.4	714.2	7218.5098	10000	0.1753	0.02408	9023.1	9.0231E5	3.383E-3	0.6	3.1	184.000	179.27	137.8
55.84	167.1	0.3342	34.000	22.4	724.1	7330.8501	10000	0.1777	0.02593	9163.6	9.1636E5	3.383E-3	0.6	3.1	185.000	171.33	133.7
52.65	161.8	0.3253	35.012	22.4	720.0	7443.2402	10000	0.1767	0.02749	9304.1	9.3041E5	3.384E-3	0.6	3.1	186.012	161.54	129.5
48.55	153.7	0.3158	36.016	22.4	743.2	7605.0298	10000	0.1824	0.03144	9506.3	9.5063E5	3.384E-3	0.6	3.1	187.016	148.94	123.0
46.23	148.6	0.3111	37.000	22.4	734.9	7705.1201	10000	0.1804	0.03326	9631.4	9.6314E5	3.383E-3	0.6	3.1	188.000	141.84	118.9
42.91	143.4	0.2994	38.000	22.4	746.5	7804.4399	10000	0.1832	0.03632	9755.6	9.7556E5	3.384E-3	0.6	3.2	189.000	131.66	114.7
39.81	135.2	0.2944	39.000	22.4	733.2	7947.5801	10000	0.1800	0.04009	9934.5	9.9345E5	3.384E-3	0.7	3.2	190.000	122.13	108.2
36.65	130.1	0.2816	40.016	22.4	753.1	8034.7900	10000	0.1848	0.04446	10043	1.0043E6	3.384E-3	0.7	3.2	191.016	112.43	104.1
35.02	124.9	0.2805	41.004	22.4	758.9	8121.8501	10000	0.1863	0.04868	10152	1.0152E6	3.384E-3	0.7	3.2	192.004	107.45	99.89
31.40	116.7	0.2691	42.000	22.4	748.1	8246.1396	10000	0.1836	0.05493	10308	1.0308E6	3.384E-3	0.7	3.2	193.000	96.344	93.36
28.87	111.6	0.2586	43.020	22.4	741.5	8320.7100	10000	0.1820	0.05949	10401	1.0401E6	3.384E-3	0.7	3.2	194.020	88.571	89.32
26.87	106.4	0.2526	44.004	22.4	752.3	8395.2803	10000	0.1846	0.06651	10494	1.0494E6	3.383E-3	0.7	3.3	195.004	82.436	85.08
24.68	97.90	0.2521	45.016	22.4	758.9	8507.3701	10000	0.1863	0.07919	10634	1.0634E6	3.383E-3	0.8	3.3	196.016	75.721	78.32
21.19	92.61	0.2289	46.016	22.4	753.9	8568.9102	10000	0.1850	0.08791	10711	1.0711E6	3.383E-3	0.8	3.3	197.016	65.024	74.08
19.08	87.27	0.2186	47.000	22.4	760.5	8630.8496	10000	0.1867	0.09986	10789	1.0789E6	3.383E-3	0.8	3.3	198.000	58.536	69.82
17.44	81.60	0.2138	48.000	22.4	752.3	8692.5996	10000	0.1846	0.1130	10866	1.0866E6	3.384E-3	0.8	3.3	199.000	53.513	65.28
14.28	73.27	0.1948	49.000	22.4	773.7	8772.9004	10000	0.1899	0.1441	10966	1.0966E6	3.383E-3	0.8	3.3	200.000	43.802	58.62
12.75	67.86	0.1878	50.016	22.4	777.1	8822.2402	10000	0.1907	0.1687	11028	1.1028E6	3.384E-3	0.8	3.4	201.016	39.103	54.29
10.84	61.99	0.1749	51.016	22.4	769.6	8871.3604	10000	0.1889	0.2003	11089	1.1089E6	3.384E-3	0.9	3.4	202.016	33.263	49.59
9.232	55.96	0.1650	52.000	22.4	779.5	8914.2803	10000	0.1913	0.2489	11143	1.1143E6	3.384E-3	0.9	3.4	203.000	28.325	44.77
7.859	50.61	0.1553	53.000	22.4	777.1	8951.5996	10000	0.1907	0.3033	11190	1.1190E6	3.384E-3	0.9	3.4	204.000	24.112	40.49
6.313	44.66	0.1414	54.016	22.4	779.5	8988.7002	10000	0.1913	0.3909	11236	1.1236E6	3.384E-3	0.9	3.4	205.016	19.369	35.73
4.734	37.83	0.1251	55.000	22.4	778.7	9023.7998	10000	0.1911	0.5441	11280	1.1280E6	3.384E-3	0.9	3.4	206.000	14.524	30.26
3.646	31.82	0.1146	56.004	22.4	768.8	9047.9297	10000	0.1887	0.7593	11310	1.1310E6	3.384E-3	0.9	3.5	207.004	11.184	25.46
2.623	25.35	0.1035	57.000	22.4	782.0	9071.7500	10000	0.1919	1.217	11340	1.1340E6	3.384E-3	1.0	3.5	208.000	8.0467	20.28
1.498	18.14	0.08258	58.016	22.4	779.5	9089.0801	10000	0.1913	2.369	11361	1.1361E6	3.384E-3	1.0	3.5	209.016	4.5956	14.51
0.7158	12.23	0.05855	59.016	22.4	779.5	9100.3896	10000	0.1913	5.216	11375	1.1375E6	3.384E-3	1.0	3.5	210.016	2.1961	9.780
0.3672	8.112	0.04527	60.016	22.4	781.2	9105.2197	10000	0.1917	11.87	11382	1.1382E6	3.384E-3	1.0	3.5	211.016	1.1266	6.490

